Читать книгу Small-Angle Scattering - Ian W. Hamley - Страница 2
Table of Contents
Оглавление1 Cover
2 Professor Ian Hamley's Book Publications
5 Preface
6 1 Basic Theory 1.1 INTRODUCTION 1.2 WAVENUMBER AND SCATTERING AMPLITUDE 1.3 INTENSITY FOR ANISOTROPIC AND ISOTROPIC SYSTEMS AND RELATIONSHIPS TO PAIR DISTANCE DISTRIBUTION AND AUTOCORRELATION FUNCTIONS 1.4 GUINIER APPROXIMATION 1.5 FORM AND STRUCTURE FACTORS 1.6 STRUCTURE FACTORS 1.7 FORM FACTORS 1.8 FORM AND STRUCTURE FACTORS FOR POLYMERS REFERENCES
7 2 Data Analysis 2.1 INTRODUCTION 2.2 PRE-MEASUREMENT SAMPLE CONCENTRATION AND POLYDISPERSITY MEASUREMENTS 2.3 OVERVIEW: DATA REDUCTION PIPELINE 2.4 CORRECTIONS FOR SAMPLE TRANSMISSION AND OTHERS 2.5 BACKGROUND CORRECTIONS 2.6 DETECTOR CORRECTIONS, MASK FILES, AND INTEGRATION 2.7 ANISOTROPIC DATA 2.8 CALIBRATION OF Q SCALE 2.9 ABSOLUTE INTENSITY CALIBRATION 2.10 ABSORPTION 2.11 SMEARING EFFECTS 2.12 SOLUTION SAXS DATA CHECKS 2.13 POROD REGIME 2.14 KRATKY PLOTS 2.15 ZIMM PLOTS 2.16 INVARIANT AND RELATED INFORMATION CONTENT FROM SAS MEASUREMENTS 2.17 FORM FACTOR FITTING 2.18 SAS SOFTWARE REFERENCES
8 3 Instrumentation for SAXS and SANS 3.1 INTRODUCTION 3.2 SYNCHROTRON FACILITIES 3.3 NEUTRON SCATTERING FACILITIES 3.4 SYNCHROTRON SAXS INSTRUMENTATION 3.5 LABORATORY SAXS INSTRUMENTATION 3.6 SANS INSTRUMENTATION 3.7 ULTRA‐SMALL‐ANGLE SCATTERING INSTRUMENTS 3.8 STANDARD SAMPLE ENVIRONMENTS – SAXS 3.9 STANDARD SAMPLE ENVIRONMENTS – SANS 3.10 STANDARD SAMPLE ENVIRONMENTS – GISAS 3.11 MICROFOCUS SAXS AND WAXS 3.12 SPECIALIZED SAMPLE ENVIRONMENTS REFERENCES
9 4 Applications and Specifics of SAXS 4.1 INTRODUCTION 4.2 PRODUCTION OF X‐RAYS 4.3 SCATTERING PROCESSES FOR X‐RAYS 4.4 ATOMIC SCATTERING FACTORS 4.5 ANOMALOUS SAXS AND SAXS CONTRAST VARIATION 4.6 BIOSAXS: SOLUTION SAXS FROM BIOMACROMOLECULES, ESPECIALLY PROTEINS 4.7 SOLUTION SAXS FROM MULTI‐DOMAIN AND FLEXIBLE MACROMOLECULES 4.8 SOLUTION SAXS FROM MULTI‐COMPONENT SYSTEMS – BIOMOLECULAR ASSEMBLIES 4.9 PROTEIN STRUCTURE FACTOR SAXS 4.10 SAXS (AND WAXS) STUDIES OF SOFT MATTER SYSTEMS 4.11 SAXS AND WAXS FROM SEMICRYSTALLINE POLYMERS 4.12 LIPID PHASES: ELECTRON DENSITY PROFILE RECONSTRUCTION 4.13 SAXS STUDIES OF PEPTIDE AND LIPOPEPTIDE ASSEMBLIES 4.14 SAXS STUDIES OF THE STRUCTURE FACTOR OF COLLOIDS 4.15 SAXS AND SAXS/WAXS STUDIES OF BIOMATERIALS 4.16 FAST TIME‐RESOLVED SAXS REFERENCES
10 5 Applications and Specifics of SANS 5.1 INTRODUCTION 5.2 PRODUCTION OF NEUTRONS 5.3 DIFFERENTIAL SCATTERING CROSS‐SECTION 5.4 SCATTERING LENGTHS 5.5 SANS DATA REDUCTION CONSIDERATIONS 5.6 CONTRAST VARIATION 5.7 SINGLE MOLECULE SCATTERING FROM MIXTURES OF PROTONATED AND DEUTERATED MOLECULES 5.8 SANS FROM LABELLED POLYMERS 5.9 KINETIC SANS USING LABELLED MIXTURES 5.10 ULTRA‐SMALL‐ANGLE SANS (USANS) 5.11 SANS AND USANS (AND SAXS AND USAXS) STUDIES ON POROUS STRUCTURES 5.12 SANS ON MAGNETIC MATERIALS 5.13 SPIN‐ECHO SANS (SESANS) 5.14 COMPLEMENTARY SAXS AND SANS REFERENCES
11 6 Grazing‐Incidence Small‐Angle Scattering 6.1 INTRODUCTION 6.2 BASIC QUANTITIES: DEFINITION OF ANGLES, REFRACTIVE INDEX, AND SCATTERING LENGTH DENSITY 6.3 CHARACTERISTIC SCANS 6.4 THE DISTORTED WAVE BORN APPROXIMATION 6.5 DATA ANALYSIS 6.6 EXPERIMENTAL EXAMPLES OF GISAS DATA 6.7 EXPERIMENTAL EXAMPLES OF GIWAXS/GIXD DATA REFERENCES
12 Index
