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Jörg Flock
X-Ray Fluorescence Spectroscopy for Laboratory Applications
Читать книгу X-Ray Fluorescence Spectroscopy for Laboratory Applications - Michael Haschke, Jörg Flock - Страница 1
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Страница 1
Table of Contents
List of Tables
List of Illustrations
Guide
Pages
X-ray Fluorescence Spectroscopy for Laboratory Applications
Страница 8
Preface
About the Authors
1 Introduction
2 Principles of X-ray Spectrometry 2.1 Analytical Performance
2.2 X-ray Radiation and Their Interaction 2.2.1 Parts of an X-ray Spectrum
2.2.2 Intensity of the Characteristic Radiation
2.2.3 Nomenclature of X-ray Lines
2.2.4 Interaction of X-rays with Matter
2.2.4.1 Absorption
2.2.4.2 Scattering
2.2.5 Detection of X-ray Spectra
2.3 The Development of X-ray Spectrometry
2.4 Carrying Out an Analysis 2.4.1 Analysis Method
2.4.2 Sequence of an Analysis
2.4.2.1 Quality of the Sample Material
2.4.2.2 Sample Preparation
2.4.2.3 Analysis Task
2.4.2.4 Measurement and Evaluation of the Measurement Data
2.4.2.5 Creation of an Analysis Report
3 Sample Preparation 3.1 Objectives of Sample Preparation
3.2 Preparation Techniques 3.2.1 Preparation Techniques for Solid Samples
3.2.2 Information Depth and Analyzed Volume
3.2.3 Infinite Thickness
3.2.4 Contaminations
3.2.5 Homogeneity
3.3 Preparation of Compact and Homogeneous Materials 3.3.1 Metals
3.3.2 Glasses
3.4 Small Parts Materials
3.4.1 Grinding of Small Parts Material
3.4.2 Preparation by Pouring Loose Powder into a Sample Cup
3.4.3 Preparation of the Measurement Sample by Pressing into a Pellet
3.4.4 Preparation of the Sample by Fusion Beads 3.4.4.1 Improving the Quality of the Analysis
3.4.4.2 Steps for the Production of Fusion Beads
3.4.4.3 Loss of Ignition
3.4.4.4 Quality Criteria for Fusion Beads
3.4.4.5 Preparation of Special Materials
3.5 Liquid Samples
3.5.1 Direct Measurement of Liquids
3.5.2 Special Processing Procedures for Liquid Samples
3.6 Biological Materials
3.7 Small Particles, Dust, and Aerosols
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